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Stable isotope dilution assay for the accurate determination of tricaine in fish samples by HPLC-MS-MS
文献类型:期刊
作者:Xie, Chaonan[1]  Li, Qin[2]  Han, Gang[3]  Liu, Huan[4]  Yang, Jien[5]  Li, Jincheng[6]  
机构:[1]Chinese Acad Fishery Sci, Beijing 100141, Peoples R China.,Minist Agr, Key Lab Control Qual & Safety Aquat Prod, Beijing, Peoples R China.;
[2]Chinese Acad Fishery Sci, Beijing 100141, Peoples R China.,Minist Agr, Key Lab Control Qual & Safety Aquat Prod, Beijing, Peoples R China.;Shanghai Ocean Univ, Coll Fisheries & Life Sci, Shanghai, Peoples R China.;
[3]Chinese Acad Fishery Sci, Beijing 100141, Peoples R China.,Minist Agr, Key Lab Control Qual & Safety Aquat Prod, Beijing, Peoples R China.;
[4]Chinese Acad Fishery Sci, Beijing 100141, Peoples R China.,Minist Agr, Key Lab Control Qual & Safety Aquat Prod, Beijing, Peoples R China.;
[5]Henan Normal Univ, Coll Phys & Mat Sci, Xinxiang, Peoples R China.,Henan Key Lab Photovolta Mat, Xinxiang, Peoples R China.;
[6]Chinese Acad Fishery Sci, Beijing 100141, Peoples R China.,Minist Agr, Key Lab Control Qual & Safety Aquat Prod, Beijing, Peoples R China.;
通讯作者:Li, JC (reprint author), Chinese Acad Fishery Sci, Beijing 100141, Peoples R China.
年:2019
期刊名称:BIOMEDICAL CHROMATOGRAPHY影响因子和分区
卷:33
期:5
增刊:正刊
收录情况:SCI(E)(WOS:000467964700010)  
语言:外文
ISSN:0269-3879
人气指数:4
浏览次数:4
基金:Central Public-interest Scientific Institution Basal Research Fund, Chinese Academy of Fishery Sciences [2018C005]
关键词:fish samples; high-performance liquid chromatography-triple quadrupole mass spectrometry; stable isotope dilution assay; tricaine
摘要:
Tricaine methanesulfonate is one of most commonly used anesthetics in fish during blood sampling, artificial propagation and long-distance transportation. In this study, an accurate method for the quantitative determination of tricaine in fish samples by a stable isotope dilution assay coupled with high-performance liquid chromatography-triple quadrupole mass spectrometry was developed. Tricaine-D-5 was synthesized and used as an isotopically labeled internal standard for the determination of tr ...More
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